Marvel Ultimate Graphic Novel Collection Issue 78 : Ultimate Spider-Man - The Death of Spider-Man

Six of Spider-Man's most dangerous foes — Norman Osborn, Dr Otto Octavius, Kraven the Hunter, Electro, the Sandman and the Vulture — have escaped from S.H.I.E.L.D. custody. United by a hatred of the wall-crawler, this sinister group are determined to make Peter Parker pay for all their past defeats. With those he holds dearest in their sights, the Ultimate Spider-Man may have to make the ultimate sacrifice to stop these insane villains once and for all.

Collecting Ultimate Spider-Man #153–160